1/2″-300LB 2-Piece Open Die Forged Cryogenic Ball Valve

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Description

TECHNICAL DATA SHEET

Forged Stainless Steel Cryogenic Floating Ball Valve
Series: DQ41F/Y / DQ61F/Y
Models: Reduced Bore / Full Bore, Side-Entry (Split Body)


1. PRODUCT OVERVIEW

This forged stainless steel cryogenic ball valve is specifically engineered for reliable shut-off and flow control of liquefied gases and cryogenic fluids down to -196°C. Designed in accordance with BS 6364, ISO 28921-1, and MSS SP-134 standards, it features a two-piece bolted body construction with extended bonnet and fully forged austenitic stainless steel components (ASTM A182 F304/F304L/F316L) to eliminate porosity and ensure structural integrity under extreme thermal cycling .

Key Features:

  • 100% Forged Body Construction: ASTM A182 F304/F304L stainless steel, no cast defects, superior low-temperature impact toughness .

  • Extended Bonnet (Long Neck): Minimum 250mm neck length for DN50 and above, positions stem packing at ambient temperature, prevents ice formation, and allows insulation application .

  • Cryogenic Stabilization Treatment: All pressure-containing parts undergo deep cryogenic treatment (LN₂ immersion, -196°C soak for 2-6 hours, 2-3 cycles) to stabilize microstructure and relieve machining stresses .

  • Blow-out Proof Stem: Integrally forged stem with anti-blowout shoulder, anti-static device (spring-loaded contact) per ISO 28921-1 .

  • Low Emission Packing: Live-loaded disc spring + graphite/RPTFE packing system, meets ISO 15848-1 Class B fugitive emission requirements .

  • Cavity Pressure Relief: Upstream seat is pressure-relieving design to prevent body cavity over-pressurization due to cryogenic fluid vaporization .

  • Full Traceability: Positive Material Identification (PMI) and EN 10204 Type 3.1 material certification available .


2. DESIGN STANDARDS & SPECIFICATIONS

Item Standard / Code
Design & Manufacture BS 6364, ISO 28921-1, MSS SP-134, ASME B16.34
Face-to-Face Dimension BS 6364 Table 1, ISO 5752 Series 11 (Extended)
End Connections ASME B16.5 (RF/RTJ), EN 1092-1, GB/T 9113, JB/T 79
Butt Weld Ends ASME B16.25, GB/T 12224
Socket Weld / Thread ASME B16.11, NPT/BSPT per ISO 7-1
Pressure Testing API 598, ISO 5208, BS 6364 Annex A (Cryogenic)
Fugitive Emission ISO 15848-1 Class B
Fire Safe (Optional) API 607 / ISO 10497
Anti-Static ISO 28921-1, BS 5353
NACE MR0175 / ISO 15156 (Optional)
SIL Rating SIL 3 Capable (IEC 61508)

3. GENERAL TECHNICAL PARAMETERS

Parameter Specification
Valve Type Floating Ball, Side-Entry (2-Piece Split Body), Anti-blowout Stem
Size Range DN15 ~ DN300 (½” ~ 12″)
Pressure Classes ASME Class 150, 300, 600 (PN16 ~ PN100)
Temperature Range -196°C ~ +80°C (Standard Cryogenic)
-196°C ~ +200°C (High Temp Option, consult factory)
Design Temperature -196°C (Liquid Nitrogen)
Minimum Design Temp -196°C (316L), -101°C (LC3), -46°C (LCB)
Service Media LNG, LN₂, LO₂, LAr, LHe, Ethylene, Liquid Propane, Ammonia, CO₂, Hydrogen
Flow Pattern Full Bore (Regular) / Reduced Bore (Optional)
Flow Direction Uni-directional (Standard), Bi-directional (Optional)
Operation Manual (Lever/Gear), Pneumatic (DA/SR), Electric
Mounting ISO 5211 top flange for direct actuator mounting
Insulation Extended bonnet suitable for cold box installation

4. MATERIALS OF CONSTRUCTION (FORGED STAINLESS STEEL)

Component Material (ASTM) Notes
Body Halves A182 F304/F304L (Forged) Carbon ≤ 0.03%, cryogenic stabilization treated, -196°C impact ≥ 50J
Bonnet (Extension) A182 F304/F304L (Forged) Extended length per BS 6364, integrally forged or welded construction
Ball A182 F304/F304L (Forged) Chrome-nickel austenitic, surface Ra ≤ 0.4μm, floating design
Stem A182 F304/F304L/F316L (Forged) Anti-blowout shoulder, cryogenic nitrogen hardening optional
Seat Rings RPTFE (Glass/Carbon Fiber Reinforced) / PCTFE / PEEK Spring-energized for low-temp sealing
Seal Carrier A182 F304/F304L
Stem Packing Graphite Foil + RPTFE, Live-loaded with Belleville springs Low emission, ISO 15848-1 Class B
Gaskets Spiral Wound (SS316L/Graphite)
Body Bolting ASTM A193 B8M Class 2 (Stainless) High strength, low-temperature compatible
Nuts ASTM A194 8M
Thrust Washer RPTFE / PTFE + Bronze Anti-extrusion, low friction
Anti-Static Device SS316L Spring + Plunger Resistance ≤ 10Ω
Handle / Gearbox SS304 / Ductile Iron

Alternative Forged Materials (Upon Request):

  • A182 F316/F316L: Enhanced pitting corrosion resistance

  • A182 F321: Stabilized grade for higher intermittent temperatures

  • Inconel 625 / Hastelloy C-276: For extreme low temp (< -196°C) + high corrosion

  • A352 LC3 / LCB: Cast low carbon steel (not forged, for non-SS requirements)


5. CRYOGENIC TREATMENT & TESTING

Cryogenic Stabilization Process:

  1. All rough-machined forged components (body, bonnet, ball, stem) are immersed in liquid nitrogen (-196°C).

  2. Soaking time: 2-6 hours depending on mass (minimum 2 hours per cycle) .

  3. Components are returned to ambient temperature naturally (no forced heating).

  4. Process repeated for minimum 2 cycles .

  5. Final precision machining after stabilization to ensure dimensional stability at cryogenic service.

Purpose:

  • Transforms retained austenite

  • Relieves residual stresses from forging/welding

  • Prevents dimensional changes and seal leakage during thermal cycling

Impact Testing:

  • Charpy V-Notch test per ASTM A370

  • Acceptance criteria: ≥ 41J (average) at -196°C for F304L

  • AOKAVI standard: ≥ 50J at -196°C


6. DIMENSIONS & CONNECTIONS (ASME CLASS 150/300 – REFERENCE)

6.1 Flanged Type (DQ41F/Y) – PN16/PN40 / Class 150/300

Unit: mm (Reference dimensions – subject to manufacturer design)

DN Size (in) L (RF) L (RTJ) D (Class 150) D (Class 300) Bonnet Extension H Approx. Weight (kg)
15 ½” 130 140 95 95 230 3.0
20 ¾” 140 152 105 105 260 4.0
25 1″ 150 165 115 115 280 5.0
32 1¼” 165 178 135 135 290 9.0
40 1½” 180 190 145 145 320 11.0
50 2″ 203 216 160 165 340 15.0
65 2½” 222 241 180 190 370 19.0
80 3″ 241 283 195 210 400 27.0
100 4″ 305 305 215 255 450 38.0
150 6″ 394 403 280 320 550 81.0
200 8″ 457 502 345 380 680 95.0
250 10″ 533 568 405 445 790 140.0
300 12″ 610 648 485 520 890 200.0

Notes:

  • Flange drilling per ASME B16.5 (Class 150 / 300). For PN16/PN40, dimensions vary per EN 1092-1.

  • Bonnet extension length per BS 6364: Minimum 250mm for DN50 and above; actual H dimension includes operator clearance .

  • Weight shown for Class 150 carbon steel body; SS body slightly heavier.


6.2 Socket Weld / Threaded Type (DQ61F/Y) – NPT/BSPT/SW

Unit: mm

DN Inch L d (Bore) D (Socket) D1 (Thread) H (Extension) W (Handle)
15 ½” 92 13 36 21.8 230 160
20 ¾” 111 18 42 27.3 260 220
25 1″ 127 23 52 33.8 280 220
32 1¼” 140 28 60 42.6 290 250
40 1½” 152 35 68 48.7 320 250
50 2″ 178 45 80 61.2 340 350

Source: 


7. PRESSURE-TEMPERATURE RATING

Forged A182 F304/F304L – ASME B16.34

Temperature (°C) Class 150 (psi) Class 300 (psi) Class 600 (psi)
-29 to +38 285 740 1480
+50 270 705 1410
+100 235 615 1230
-196°C (Derated) 230 600 1200

Critical Notes:

  • Floating ball design is limited to Class 300 maximum due to stem thrust loading .

  • For Class 600 and above, trunnion-mounted cryogenic ball valve design is required.

  • Pressure rating at -196°C is derated per ASME B16.34 and BS 6364 requirements .


8. PERFORMANCE & LEAKAGE TESTS

Test Type Standard Criteria
Shell Hydrostatic Test API 598 / ISO 5208 1.5 × rated pressure at ambient, no visible leakage
High-Pressure Pneumatic Test API 598 0.6 MPa (80 psi) air, soap bubble test
Cryogenic Seat Leakage Test BS 6364 Annex A Valve immersed in LN₂ (-196°C), 1.1× rated pressure, max leakage: 0.1 Nm³/hr × DN (mm) for gas
High-Performance Cryogenic Leakage AOKAVI / ISO 28921-1 ≤ 1×10⁻⁹ mL/min (Helium) at -196°C
Fugitive Emission (Stem) ISO 15848-1 Class B ≤ 10⁻⁵ mbar·L/s (Helium)
Anti-Static Test ISO 28921-1 Resistance ≤ 10Ω between stem and body
Fire Safe (Optional) API 607 Per API 607 7th Edition

9. OPERATING TORQUE (REFERENCE @ -196°C)

DN Size Torque (N·m) @ ΔP=40 bar Actuator Recommendation
15 ½” 8 – 12 Manual Lever / Small Pneumatic
25 1″ 20 – 30 Manual Lever
50 2″ 80 – 120 Manual Lever / Gear
80 3″ 180 – 250 Gear / Pneumatic
100 4″ 300 – 400 Gear / Pneumatic
150 6″ 700 – 900 Gearbox / Pneumatic

Notes:

  • Torque increases significantly with pressure differential and seat material (PCTFE higher than RPTFE).

  • Safety factor for actuator sizing: 1.3 – 1.5 for pneumatic, 1.5 – 2.0 for electric .

  • Values shown for RPTFE seats, clean media, DN50 tested per .


10. DESIGN FEATURES & CRYOGENIC SPECIALTIES

Extended Bonnet (Long Neck):

  • Mandatory for service below -50°C .

  • Positions stem packing and actuator at ambient temperature zone.

  • Prevents ice formation and lubrication solidification.

  • Standard neck length: 250mm for DN50, scaled proportionally for other sizes.

Pressure Relief Mechanism:

  • Floating ball design inherently allows upstream seat to act as pressure relief.

  • Prevents body cavity overpressure due to liquid vaporization (cryogenic pumping effect) .

  • For fixed ball designs, optional internal relief valve or self-relieving seat.

Anti-Static Device:

  • Required per ISO 28921-1 and BS 5353 for flammable cryogenic media (LNG, ethylene, etc.).

  • Spring-loaded plunger continuously grounds ball to body.

Oxygen Service Cleaning:

  • Optional degreasing and cleaning per CGA G-4.1 (for liquid oxygen service).

  • Chlorine-free packaging and labeling .


11. APPLICATIONS & INDUSTRY USE

Industry Typical Media Temperature
LNG / LPG Methane, Ethane, Propane, Butane -162°C to -46°C
Industrial Gases (Air Separation) Liquid Nitrogen (LN₂), Liquid Oxygen (LO₂), Liquid Argon (LAr) -196°C to -183°C
Hydrogen Energy Liquid Hydrogen (LH₂) -253°C (Inconel/Ti req’d)
Petrochemical Ethylene, Propylene -104°C
Refrigeration Ammonia (R717), CO₂ (R744) -46°C to -78°C
Cryogenic Storage Liquid Helium (LHe) -269°C (Special alloy)
Aerospace Rocket propellants (LO₂, LH₂) -253°C to -183°C
Pharmaceutical / Biotech Liquid nitrogen freezing -196°C

12. QUALIFICATION & CERTIFICATION

Certification Scope Availability
BS 6364 Cryogenic valve design & testing Standard
ISO 28921-1 Industrial cryogenic valves Standard
PED 2014/68/EU Category III, Module H Optional
TA-Luft (VDI 2440) Fugitive emission Optional
API 607 Fire safe testing Optional
NACE MR0175 Sour service Optional
ATEX 2014/34/EU Explosive atmospheres (Zone 1/2) Optional
ISO 9001:2015 Quality management Standard
EN 10204 3.1/3.2 Material certification Optional

13. SELECTION & ORDERING INFORMATION

To ensure correct valve selection for your cryogenic application, please specify:

  1. Model: DQ41F (Flanged) / DQ61F (SW/NPT) / DQ47F (Gear)

  2. Size (DN/NPS): e.g., DN50 (2″)

  3. Pressure Class: Class 150 / 300 / PN16 / PN40

  4. Body MaterialA182 F304/F304L (Forged SS) — standard for -196°C

  5. Ball/Stem Material: A182 F304/F304L

  6. Seat Material: RPTFE / PCTFE / PEEK (specify)

  7. End Connection: RF flange, RTJ flange, NPT, BSPT, SW, BW

  8. Design Temperature: -196°C / -101°C / -46°C

  9. Service Media: LNG / LN₂ / LO₂ / Ethylene / Other (specify)

  10. Operation: Manual Lever / Gear / Pneumatic / Electric

  11. Special Requirements:

    • Cryogenic test with BS 6364 certificate

    • Oxygen cleaning (CGA G-4.1)

    • Anti-static device

    • Fire-safe design (API 607)

    • NACE MR0175

    • Extended bonnet length (custom)

    • PMI testing

    • EN 10204 3.1 material certs